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pd_meltingpoint:95-99 °C
Purity:99%
InChI:InChI=1/C11H18BNO3/c1-7-9(8(2)14-13-7)12-15-10(3,4)11(5,6)16-12/h1-6H3
A transition-metal-free method has been ...
4-bromo-3,5-dimethyl-1,2-oxazole
dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane
3,5-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isoxazole
3,5-dimethyl-4-dimethylphenylsilylisoxazole
| Conditions | Yield |
|---|---|
|
dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane;
With
potassium methanolate;
In
1,2-dimethoxyethane;
at 30 ℃;
for 0.166667h;
4-bromo-3,5-dimethyl-1,2-oxazole;
In
1,2-dimethoxyethane;
at 30 ℃;
for 1h;
Overall yield = 57 %;
|
51% |
3,5-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isoxazole
water
3,5-dimethylisoxazole-4-boronic acid
2,3-dimethyl-2,3-butane diol
| Conditions | Yield |
|---|---|
|
In
1,4-dioxane;
at 26.84 ℃;
Kinetics;
Equilibrium constant;
|
4-bromo-3,5-dimethyl-1,2-oxazole
dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane
C14H15NO3
N-(2,4-difluorophenyl)-5-(3,5-dimethylisoxazol-4-yl)pyrido[3,2-d]pyridazin-2-amine
4-(3,5-dimethylisoxazol-4-yl)benzamide
4-mesityl-3,5-dimethylisoxazole
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