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Purity:99%
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(Z)-cyclooct-2-enone
(Z)-2-cycloocten-1-ol
(+/-)-(E)-(1R,2R)-cyclo-oct-2-en-1-ol
| Conditions | Yield |
|---|---|
|
With
lithium aluminium tetrahydride;
Yield given. Multistep reaction. Yields of byproduct given;
1.) diethyl ether, irradiation, 0 deg C, 1.5 h, 2.) 0 deg C, 10 min; room temperature, 20 min;
|
axial-(E)-cyclooct-2-en-1-ol
benzyl bromide
C12H18N2
benzyl alcohol
| Conditions | Yield |
|---|---|
|
Multi-step reaction with 2 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 5 h / 20 - 55 °C
1.2: 96 h
2.1: chloroform / 1 h / 20 °C
With
sodium hydride;
In
tetrahydrofuran; chloroform; mineral oil;
|
(Z)-cyclooct-2-enone
C12H18N2
1,3-Diphenylpropanone
benzyl alcohol
(E)-cyclooct-2-en-1-yl-(4-nitrophenyl)carbonate
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