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83321-23-7

  • Product Name:1,1-Bis(iodomethyl)cyclopropane
  • Molecular Weight:321.928
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Product Details

Purity:99%

Bulk supply high purity 1,1-Bis(iodomethyl)cyclopropane 83321-23-7, Paid sample available

  • Molecular Formula:
  • Molecular Weight:321.928
  • Vapor Pressure:0.026mmHg at 25°C 
  • Boiling Point:255.476°C at 760 mmHg 
  • Flash Point:122.297°C 
  • Density:2.449g/cm3 

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83321-23-7 Process route

[1-(hydroxymethyl)cyclopropyl]methanol
39590-81-3

[1-(hydroxymethyl)cyclopropyl]methanol

1,1-bis(iodomethyl)cyclopropane
83321-23-7

1,1-bis(iodomethyl)cyclopropane

Conditions
Conditions Yield
With 1H-imidazole; iodine; triphenylphosphine; In dichloromethane; at 0 - 20 ℃; for 2.5h;
96%
With chloro-trimethyl-silane; sodium iodide; In acetonitrile; for 16h; Ambient temperature;
80%
With 1H-imidazole; iodine; triphenylphosphine; In dichloromethane; at 0 - 10 ℃; for 2.5h;
70%
With 1H-imidazole; iodine; triphenylphosphine; In dichloromethane; at 10 ℃; for 3h;
70%
With 1H-imidazole; iodine; triphenylphosphine; In dichloromethane; at 0 - 15 ℃; for 3.5h;
46%
Multi-step reaction with 2 steps
2: acetone; sodium iodide
With acetone; sodium iodide;
Multi-step reaction with 2 steps
1: triethylamine / acetone / 3 h / 0 - 20 °C
2: sodium iodide / acetone / 35 °C
With triethylamine; sodium iodide; In acetone;
With 1H-imidazole; iodine; triphenylphosphine; In chlorosulfonic acid; at -10 - 20 ℃; for 3h; Inert atmosphere;
cyclopropane-1,1-diylbis(methylene) dimethanesulfonate
136476-38-5

cyclopropane-1,1-diylbis(methylene) dimethanesulfonate

1,1-bis(iodomethyl)cyclopropane
83321-23-7

1,1-bis(iodomethyl)cyclopropane

Conditions
Conditions Yield
With sodium iodide; In acetone; at 35 ℃;
94%

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