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pd_meltingpoint:30-35°C
Purity:99%
Heterogeneous photocatalysis is increasi...
There has been a continuous effort towar...
Fluorescent polymersomes with both aggre...
A series of dodecyl-based monofunctional...
carbon disulfide
bis(dodecylsulfanylthiocarbonyl)disulfide
| Conditions | Yield |
|---|---|
|
1-dodecylthiol;
With
potassium tert-butylate;
In
tetrahydrofuran; n-heptane;
at 5 - 10 ℃;
for 0.5h;
carbon disulfide;
In
tetrahydrofuran; n-heptane;
at 5 - 23 ℃;
for 4.5h;
With
iodine;
In
tetrahydrofuran; n-heptane;
at 16 - 20 ℃;
for 15.6667h;
|
98% |
carbon disulfide
1-dodecylthiol
bis(dodecylsulfanylthiocarbonyl)disulfide
| Conditions | Yield |
|---|---|
|
1-dodecylthiol;
With
sodium hydride;
In
diethyl ether; mineral oil;
at 5 ℃;
for 0.166667h;
carbon disulfide;
With
iodine;
In
diethyl ether;
at 0 - 20 ℃;
for 1h;
|
83% |
|
carbon disulfide; 1-dodecylthiol;
With
potassium hydroxide; Aliquat 336;
In
water;
at 20 ℃;
for 0.5h;
With
p-toluenesulfonyl chloride;
In
water;
at -5 - 45 ℃;
for 1.25h;
|
81% |
|
1-dodecylthiol;
With
potassium tert-butylate;
In
tetrahydrofuran; n-heptane;
at 5 - 15 ℃;
for 0.916667h;
carbon disulfide;
In
tetrahydrofuran; n-heptane;
at 5 - 20 ℃;
for 5.75h;
With
iodine;
In
tetrahydrofuran; n-heptane;
at 20 ℃;
for 14.5h;
|
3.7 g |
|
carbon disulfide; 1-dodecylthiol;
With
sodium hydroxide;
In
diethyl ether;
With
iodine;
In
diethyl ether;
at 20 ℃;
for 1h;
|
carbon disulfide
1-dodecylthiol
sodium dodecanethiolate
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