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Purity:99%
The invention discloses a substrate name...
C24H26ClNO11
6-chloro-3-indol-α-D-glucopyranoside
| Conditions | Yield |
|---|---|
|
With
sodium methylate;
In
methanol;
|
62% |
α-D-glucopyranose peracetylate
6-chloro-3-indol-α-D-glucopyranoside
| Conditions | Yield |
|---|---|
|
Multi-step reaction with 4 steps
1: acetonitrile / 12 h / 20 °C
2: potassium carbonate / dichloromethane / 6 h / 20 °C / Inert atmosphere
3: boron trifluoride diethyl etherate / dichloromethane / 9 h / 20 °C / Inert atmosphere
4: sodium methylate / methanol
With
boron trifluoride diethyl etherate; sodium methylate; potassium carbonate;
In
methanol; dichloromethane; acetonitrile;
|
α-D-glucopyranose peracetylate
2,3,4,6-tetraacetylglucose
O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)trichloroacetimidate
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