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Purity:99%
In this paper, a new series of novel aro...
In this paper, 2,7-dihydroxy-9,9-bis(4-a...
A new cardanol containing tetra-function...
The invention provides N-semi aromatic h...
2,7-dihydroxy-9H-fluoren-9-one
aniline
9,9-bis(4-aminophenyl)-2,7-dihydroxyfluorenone
Conditions | Yield |
---|---|
With
trifluorormethanesulfonic acid;
at 150 ℃;
for 10h;
Inert atmosphere;
|
92.3% |
With
methanesulfonic acid;
at 150 ℃;
for 10h;
|
86% |
With
aniline hydrochloride;
at 180 ℃;
for 1h;
|
73.6% |
With
methanesulfonic acid;
at 150 ℃;
for 10h;
|
|
With
methanesulfonic acid;
at 150 ℃;
for 14h;
|
9-oxo-9H-fluorene-2,7-diyl diacetate
9,9-bis(4-aminophenyl)-2,7-dihydroxyfluorenone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps
1: 97.6 percent / aq. KOH / 2 h / Heating
2: 73.6 percent / aniline hydrochloride / 1 h / 180 °C
With
potassium hydroxide; aniline hydrochloride;
|
2,7-dihydroxy-9H-fluoren-9-one
aniline
9-oxo-9H-fluorene-2,7-diyl diacetate
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