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pd_meltingpoint:110-112℃
Purity:99%
InChI:InChI=1/C9H5BrClN/c10-6-1-2-9-7(5-6)8(11)3-4-12-9/h1-5H
Disclosed herein are quinoline-based com...
The invention discloses a 6-bromo-4-chlo...
The invention belongs to the field of me...
The present invention provides for a met...
6-bromoquinolin-4-ol
6-bromo-4-chloroquinoline
| Conditions | Yield |
|---|---|
|
With
trichlorophosphate;
for 6h;
Heating / reflux;
|
98.5% |
|
With
trichlorophosphate;
for 2h;
Reflux;
|
93% |
|
With
trichlorophosphate;
for 1.5h;
Reflux;
|
93% |
|
With
trichlorophosphate;
In
N,N-dimethyl-formamide;
at 120 ℃;
for 5h;
|
84% |
|
6-bromoquinolin-4-ol;
With
trichlorophosphate;
Heating / reflux;
With
water;
|
84% |
|
With
trichlorophosphate;
In
toluene;
at 115 ℃;
for 4h;
|
32% |
|
With
trichlorophosphate;
In
toluene;
at 115 ℃;
for 4h;
|
32% |
|
With
trichlorophosphate;
at 135 ℃;
|
|
|
With
trichlorophosphate;
for 1.5h;
Reflux;
|
|
|
With
trichlorophosphate;
at 20 ℃;
for 19h;
|
|
|
With
trichlorophosphate;
In
N,N-dimethyl-formamide;
for 6h;
Reflux;
Inert atmosphere;
|
|
|
With
trichlorophosphate;
for 24h;
Reflux;
|
|
|
With
trichlorophosphate;
for 1.5h;
Reflux;
|
|
|
With
trichlorophosphate;
for 1.5h;
Reflux;
|
|
|
With
trichlorophosphate;
for 1.5h;
Reflux;
|
6-bromo-3-quinolinecarboxylic acid-4-ol
6-bromo-4-chloroquinoline
| Conditions | Yield |
|---|---|
|
With
trichlorophosphate;
for 2h;
Reflux;
|
99% |
|
With
phosphorus trichloride;
In
toluene;
for 2h;
Concentration;
Reflux;
|
92.6% |
|
With
thionyl chloride;
N,N-dimethyl-formamide;
for 3h;
Heating / reflux;
|
85% |
|
With
trichlorophosphate;
In
N,N-dimethyl-formamide;
for 2h;
Reflux;
|
70% |
6-bromoquinolin-4-ol
N-(2-acetyl-4-bromophenyl)acetamide
N,N-dimethyl-formamide
6-bromo-4-hydroxyquinoline-3-carboxylic acid
4-chloro-6-(4-chlorophenyl)quinoline
4-chloro-6-(4-methoxyphenyl)quinoline
tert-butyl 4-(6-bromoquinolin-4-yl)piperazine-1-carboxylate
4-chloroquinoline-6-carbaldehyde
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