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pd_meltingpoint:169 °C
Purity:99%
InChI:InChI=1/C6H4O3S/c7-3-4-1-2-5(10-4)6(8)9/h1-3H,(H,8,9)/p-1
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5-formyl-thiophene-2-carboxylic acid methyl ester
5-formyl-2-thiophencarboxylic acid
Conditions | Yield |
---|---|
With
potassium hydroxide; water;
In
tetrahydrofuran;
|
59% |
2-(2-thienyl)-1,3-dioxolane
carbon dioxide
5-formyl-2-thiophencarboxylic acid
Conditions | Yield |
---|---|
2-(2-thienyl)-1,3-dioxolane;
With
n-butyllithium; N,N,N,N,-tetramethylethylenediamine;
In
tetrahydrofuran; hexane;
at -78 ℃;
for 2h;
carbon dioxide;
In
tetrahydrofuran; hexane;
at -78 - 20 ℃;
|
88% |
2-(2-thienyl)-1,3-dioxolane;
With
n-butyllithium;
In
tetrahydrofuran;
at -78 ℃;
carbon dioxide;
With
sulfuric acid;
In
tetrahydrofuran; water;
|
|
2-(2-thienyl)-1,3-dioxolane;
With
n-butyllithium;
In
tetrahydrofuran;
at -78 ℃;
carbon dioxide;
With
sulfuric acid;
|
carbon dioxide
1,3-dimethyl-2-(thiophen-2-yl)imidazolidine
thiophene-2-carbaldehyde
5-formyl-thiophene-2-carboxylic acid methyl ester
2-ethoxycarbonyl-thiophene-5-carboxaldehyde
3-(3-thiophene)carboxyl-1-(2,5-dimethoxyphenyl)prop-2-en-1-one
5-(2-methyl-2-methoxycarbonylpropyl)thiophene-2-carboxylic acid tert-butyl ester
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