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pd_meltingpoint:106.0 to 110.0 °C
Appearance:Brown solid
Purity:99%
InChI:InChI=1/C11H14N2/c1-8-9(6-7-12)10-4-2-3-5-11(10)13-8/h2-5,13H,6-7,12H2,1H3
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5-chloro-2-pentanone
phenylhydrazine
2-methyltryptamine
Conditions | Yield |
---|---|
In
ethanol;
at 80 ℃;
for 4h;
|
82% |
In
ethanol;
at 80 ℃;
for 4h;
|
80% |
In
ethanol; water;
at 75 - 150 ℃;
for 0.333333h;
Microwave irradiation;
|
76% |
In
ethanol;
at 40 ℃;
for 4.5h;
Inert atmosphere;
Reflux;
|
70.1% |
In
ethanol;
at 35 - 40 ℃;
for 4.5h;
Inert atmosphere;
|
70.1% |
In
ethanol;
for 4h;
Reflux;
|
69% |
With
ethanol;
at 35 - 81 ℃;
for 2.58333h;
Concentration;
Large scale;
|
46% |
In
ethanol;
Reflux;
|
|
In
ethanol;
Reflux;
|
|
In
water;
at 25 - 75 ℃;
for 2.16667h;
|
105 g |
In
ethanol;
at 110 ℃;
for 10h;
Inert atmosphere;
|
2-amino-1-(2-methyl-1H-indol-3-yl)ethan-1-one
2-methyltryptamine
Conditions | Yield |
---|---|
With
triethylsilane;
In
acetonitrile;
at 20 - 30 ℃;
|
76.6% |
2-(2-methyl-1H-indol-3-yl)acetonitrile
2-Methyl-3-(2-nitroethyl)-1H-indole
indole
N-Acetyltryptamine
[(E)-2-(2-Methyl-1H-indol-3-yl)-ethylimino]-acetic acid (1S,2R,5S)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester
(1S,2R,5S)-5-Methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (E)-<<2-(2-methyl-1H-indol-3-yl)ethyl>imino>acetate
(E)-3-[4-[[[2-(2-methyl-1H-indol-3-yl)ethyl]amino]methyl]phenyl]acrylic acid methyl ester
C17H15Cl2N3O2
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