pd_meltingpoint:~200 °C (dec.)
Appearance:white crystalline powder
Purity:99%
The invention belongs to the technical f...
The invention belongs to the technical f...
The invention belongs to the technical f...
The invention belongs to the field of me...
2-(trimethylsilylamino)-4-(trimethylsilyloxy)-s-triazine
1-chloro-2-deoxy-D-ribofuranose
5-aza-2'-deoxycytidine
| Conditions | Yield |
|---|---|
|
1-chloro-2-deoxy-D-ribofuranose; With cobalt(II) nitrate; 1,1'-bi-2-naphthol; In N,N-dimethyl-formamide; at 60 ℃; Inert atmosphere;
2-(trimethylsilylamino)-4-(trimethylsilyloxy)-s-triazine; With triethylamine; In N,N-dimethyl-formamide; at 40 ℃; Temperature; Concentration; Reagent/catalyst;
|
89.3% |
|
1-chloro-2-deoxy-D-ribofuranose; With (S)-(1,1'-binaphthalene)-2,2'-diylbis(diphenylphosphine); palladium dichloride; In N,N-dimethyl-formamide; at 60 ℃; Inert atmosphere;
2-(trimethylsilylamino)-4-(trimethylsilyloxy)-s-triazine; With triethylamine; In N,N-dimethyl-formamide; at 40 ℃; for 6h; Reagent/catalyst; Temperature;
|
87.2% |
1-(3,5-di-O-p-chlorobenzoyl-2-deoxy-β-D-ribofuranosyl)-5-azacytosine
5-aza-2'-deoxycytidine
| Conditions | Yield |
|---|---|
|
With ammonia; Alcoholic medium;
|
100% |
|
With methanol; sodium methylate; at 25 ℃; for 3h; Reagent/catalyst;
|
71.6% |
|
With methanol; sodium methylate; at 20 ℃; for 12h;
|
2.8 g |
|
With methanol; sodium methylate; at 65 ℃; for 6h; Inert atmosphere;
|
34.24 g |
N-(formylamidino)-N'-β-D-2-deoxyribofuranosylurea
decitabine monohydrate
5-azacytosine
3,5-O-bis(4-chlorobenzoyl)-2-deoxy-α-D-ribofuranosyl chloride
2'-deoxy-3',5'-di-O-p-toluoyl-5-azacytidine
2'-deoxy-5'-O-p-toluoyl-5-azacytidine
2'-deoxy-β-D-5-azacytidine 5'-monophosphate
2'-deoxy-N4-[2-(4-nitrophenyl)ethoxycarbonyl]-5-azacytidine
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