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pd_meltingpoint:~200 °C (dec.)
Appearance:white crystalline powder
Purity:99%
The invention belongs to the technical f...
The invention belongs to the technical f...
The invention belongs to the technical f...
The invention belongs to the field of me...
2-(trimethylsilylamino)-4-(trimethylsilyloxy)-s-triazine
1-chloro-2-deoxy-D-ribofuranose
5-aza-2'-deoxycytidine
| Conditions | Yield |
|---|---|
|
1-chloro-2-deoxy-D-ribofuranose;
With
cobalt(II) nitrate; 1,1'-bi-2-naphthol;
In
N,N-dimethyl-formamide;
at 60 ℃;
Inert atmosphere;
2-(trimethylsilylamino)-4-(trimethylsilyloxy)-s-triazine;
With
triethylamine;
In
N,N-dimethyl-formamide;
at 40 ℃;
Temperature;
Concentration;
Reagent/catalyst;
|
89.3% |
|
1-chloro-2-deoxy-D-ribofuranose;
With
(S)-(1,1'-binaphthalene)-2,2'-diylbis(diphenylphosphine); palladium dichloride;
In
N,N-dimethyl-formamide;
at 60 ℃;
Inert atmosphere;
2-(trimethylsilylamino)-4-(trimethylsilyloxy)-s-triazine;
With
triethylamine;
In
N,N-dimethyl-formamide;
at 40 ℃;
for 6h;
Reagent/catalyst;
Temperature;
|
87.2% |
1-(3,5-di-O-p-chlorobenzoyl-2-deoxy-β-D-ribofuranosyl)-5-azacytosine
5-aza-2'-deoxycytidine
| Conditions | Yield |
|---|---|
|
With
ammonia;
Alcoholic medium;
|
100% |
|
With
methanol; sodium methylate;
at 25 ℃;
for 3h;
Reagent/catalyst;
|
71.6% |
|
With
methanol; sodium methylate;
at 20 ℃;
for 12h;
|
2.8 g |
|
With
methanol; sodium methylate;
at 65 ℃;
for 6h;
Inert atmosphere;
|
34.24 g |
N-(formylamidino)-N'-β-D-2-deoxyribofuranosylurea
decitabine monohydrate
5-azacytosine
3,5-O-bis(4-chlorobenzoyl)-2-deoxy-α-D-ribofuranosyl chloride
2'-deoxy-3',5'-di-O-p-toluoyl-5-azacytidine
2'-deoxy-5'-O-p-toluoyl-5-azacytidine
2'-deoxy-β-D-5-azacytidine 5'-monophosphate
2'-deoxy-N4-[2-(4-nitrophenyl)ethoxycarbonyl]-5-azacytidine
CAS：112163-33-4
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