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852288-18-7

  • Product Name:Fmoc-DOPA(Acetonide)-OH
  • Molecular Formula:C27H25NO6
  • Molecular Weight:459.499
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Product Details

Purity:99%

Manufacturer supply high quality Fmoc-DOPA(Acetonide)-OH 852288-18-7 with ISO standards

  • Molecular Formula:C27H25NO6
  • Molecular Weight:459.499
  • Boiling Point:663.072 °C at 760 mmHg 
  • PKA:3.68±0.10(Predicted) 
  • Flash Point:354.814 °C 
  • PSA：94.09000 
  • Density:1.302g/cm3 
  • LogP:5.11920 

852288-18-7 Relevant articles

Medical intermediate compound and synthesis method thereof

-

Paragraph 0066; 0068-0069; 0071-0072; 0074, (2019/08/02)

The invention provides a medical interme...

Method of synthesizing acetonide-protected catechol-containing compounds and intermediates produced therein

-

Page/Page column 18-19; 20, (2012/07/30)

The inventors disclose here a novel, fac...

Method of Synthesizing Acetonide-Protected Catechol-Containing Compounds and Intermediates Produced Therein

-

, (2010/04/30)

The inventors disclose here a novel, fac...

Convenient synthesis of acetonide-protected 3,4-dihydroxyphenylalanine (DOPA) for Fmoc solid-phase peptide synthesis

Liu, Zhongqiang,Hu, Bi-Huang,Messersmith, Phillip B.

, p. 5519 - 5521 (2008/12/22)

We report a facile approach to the synth...

852288-18-7 Process route

H-DOPA(acetonide)-OH

H-DOPA(acetonide)-OH

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide
82911-69-1

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

(2S)-3-(2,2-dimethyl-1,3-benzodioxol-5-yl)-2-(9H-fluoren-9-ylmethoxycarbonylamino)propanoic acid
852288-18-7

(2S)-3-(2,2-dimethyl-1,3-benzodioxol-5-yl)-2-(9H-fluoren-9-ylmethoxycarbonylamino)propanoic acid

Conditions
Conditions Yield
In tetrahydrofuran; water; at 0 ℃; for 2h;
74%
H-DOPA(acetonide)-OH; N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide; In tetrahydrofuran; water; at 0 ℃; for 2h; Cooling with ice;
With hydrogenchloride; In water; pH=2 - 3;
2,2-dimethoxy-propane
77-76-9

2,2-dimethoxy-propane

N-(9-fluorenylmethyloxycarbonyl)-3,4-dihydroxy-L-phenylalanine
137018-93-0

N-(9-fluorenylmethyloxycarbonyl)-3,4-dihydroxy-L-phenylalanine

(2S)-3-(2,2-dimethyl-1,3-benzodioxol-5-yl)-2-(9H-fluoren-9-ylmethoxycarbonylamino)propanoic acid
852288-18-7

(2S)-3-(2,2-dimethyl-1,3-benzodioxol-5-yl)-2-(9H-fluoren-9-ylmethoxycarbonylamino)propanoic acid

Conditions
Conditions Yield
In toluene; at 80 ℃; for 0.416667h; under 225.023 Torr; Temperature; Reagent/catalyst; Solvent; Pressure; Inert atmosphere; Sealed tube; Molecular sieve;
90 %Chromat.

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