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pd_meltingpoint:178-183 °C
Appearance:white to slightly beige crystalline powder
Purity:99%
InChI:InChI=1/C4H6N2O/c5-3-1-7-2-4(3)6/h1-2H,5-6H2
Highly energetic 3,4-di(nitramino)furaza...
On the basis of a design strategy that r...
Azoxyfurazan derivatives based on the tr...
Energetic compounds with fused tetracycl...
Two energetic N-trinitroethyl-substitute...
Diaminofurazan (1) was synthesized from ...
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The invention relates to a tetrazine-fur...
The invention discloses a kilogram-grade...
Glyoxal
3,4-diaminofurazan
Conditions | Yield |
---|---|
With
hydroxylamine hydrochloride; urea; sodium hydroxide;
In
water;
at 105 ℃;
for 2h;
|
67% |
Glyoxal;
With
hydroxylamine hydrochloride; sodium hydroxide;
In
water;
at 108 ℃;
for 7h;
Cooling with ice;
With
urea;
In
water;
at 100 - 110 ℃;
for 24h;
Temperature;
|
50% |
With
hydroxylamine hydrochloride; urea; sodium hydroxide;
In
water;
at 110 ℃;
|
45% |
With
hydroxylamine hydrochloride; urea;
at 102 - 108 ℃;
|
|
With
hydroxylamine hydrochloride; urea;
at 102 - 108 ℃;
|
|
With
hydroxylamine hydrochloride; urea; sodium hydroxide;
at 125 ℃;
for 15h;
|
|
With
hydroxylamine hydrochloride; urea; sodium hydroxide;
at 105 ℃;
for 15h;
|
diaminoglyoxime
3,4-diaminofurazan
Conditions | Yield |
---|---|
With
potassium hydroxide;
at 170 - 180 ℃;
for 2h;
|
70% |
With
potassium hydroxide;
for 0.333333h;
microwave irradiation;
|
70% |
With
potassium hydroxide;
In
ethylene glycol;
at 120 - 170 ℃;
for 1h;
Product distribution / selectivity;
|
52% |
In
ethylene glycol;
at 165 ℃;
for 0.5h;
Product distribution / selectivity;
|
52% |
With
potassium hydroxide;
at 170 ℃;
for 2h;
|
50% |
With
sodium hydroxide;
at 165 ℃;
|
|
With
sodium hydroxide;
In
N,N-dimethyl-formamide;
for 4h;
Ambient temperature;
|
|
With
potassium hydroxide;
at 180 ℃;
|
|
at 165 ℃;
for 0.5h;
Product distribution / selectivity;
Neat (no solvent);
|
|
With
potassium hydroxide;
In
water;
|
diaminoglyoxime
5-trifluoromethyl-1,2,4-oxadiazole-3-carboxyamidoxime
3,3’-bi-(5-trifluoromethyl-1,2,4-oxadiazole)
1H-indene-1,3(2H)-dione
5-(4-chloro-phenyl)-[1,2,5]oxadiazolo[3,4-b]pyrazine
5,7-diphenyl-4H-[1,2,5]oxadiazolo[3,4-b][1,4]diazepine
5-(4-methoxyphenyl)furazano[3,4-b]pyrazine
3-amino-4-benzamidofurazan
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