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Purity:99%
The direct Pd-catalyzed ortho C-H hydrox...
A pharmaceutical compound of the formula...
2-methylphenyl aldehyde
3-hydroxy-2-methylbenzaldehyde
| Conditions | Yield |
|---|---|
|
With
palladium diacetate; toluene-4-sulfonic acid; 1-fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate; acetic acid; 2-Amino-4-chlorobenzoic acid;
at 90 ℃;
for 24h;
Sealed tube;
|
44% |
(RS)-6-Acetoxy-5,6-dimethyl-2,4-cyclohexadien-1-on
3-hydroxy-2-methylbenzaldehyde
| Conditions | Yield |
|---|---|
|
With
sodium acetate; dimethyl sulfoxide;
|
(RS)-6-Acetoxy-5,6-dimethyl-2,4-cyclohexadien-1-on
2-methylphenyl aldehyde
3-methoxy-2-methyl-benzaldehyde
3-ethoxy-2-methylbenzaldehyde
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