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4-ethyl-1-naphthalenecarboxylic acid
4-ethyl-1-naphthoyl chloride
| Conditions | Yield |
|---|---|
|
With
thionyl chloride;
for 0.25h;
Heating;
|
|
|
With
oxalyl dichloride;
In
dichloromethane;
at 0 ℃;
Reflux;
Inert atmosphere;
|
|
|
With
oxalyl dichloride;
In
N,N-dimethyl-formamide;
|
|
|
With
oxalyl dichloride; N,N-dimethyl-formamide;
In
dichloromethane;
Reflux;
|
|
|
With
oxalyl dichloride;
In
dichloromethane; N,N-dimethyl-formamide;
at 20 ℃;
for 3h;
|
N,N-diphenyl-4-ethyl-1-naphthalenecarboxamide
4-ethyl-1-naphthoyl chloride
| Conditions | Yield |
|---|---|
|
Multi-step reaction with 2 steps
1: 90 percent / KOH / bis-(2-hydroxy-ethyl) ether / 8 h / Heating
2: thionyl chloride / 0.25 h / Heating
With
potassium hydroxide; thionyl chloride;
In
diethylene glycol;
|
4-ethyl-1-naphthalenecarboxylic acid
N,N-diphenyl-4-ethyl-1-naphthalenecarboxamide
1-ethylnapthelene
JWH-210
JWH-213
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