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24880-43-1

  • Product Name:Mesembrine
  • Molecular Formula:C17H23 N O3
  • Molecular Weight:289.375
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Product Details

Purity:99%

Quality Factory Sells Top Purity 99% Mesembrine 24880-43-1 with Safe Delivery

  • Molecular Formula:C17H23NO3
  • Molecular Weight:289.375
  • Vapor Pressure:3.09E-07mmHg at 25°C 
  • Boiling Point:419.2°Cat760mmHg 
  • PKA:8.78±0.40(Predicted) 
  • Flash Point:207.3°C 
  • PSA：38.77000 
  • Density:1.133g/cm3 
  • LogP:2.33660 

Mesembrine(Cas 24880-43-1) Usage

Synthesis Reference(s)

Tetrahedron, 24, p. 6583, 1968 DOI: 10.1016/S0040-4020(01)96872-3

InChI:InChI=1/C17H23NO3/c1-18-9-8-17(7-6-13(19)11-16(17)18)12-4-5-14(20-2)15(10-12)21-3/h4-5,10,16H,6-9,11H2,1-3H3/t16-,17-/m0/s1

24880-43-1 Relevant articles

Palladium-catalyzed asymmetric direct intermolecular allylation of α-aryl cyclic vinylogous esters: Divergent synthesis of (+)-oxomaritidine and (?)-mesembrine

Wang, Wei,Dai, Jun,Yang, Qiqiong,Deng, Yu-Hua,Peng, Fangzhi,Shao, Zhihui

supporting information, p. 920 - 924 (2021/02/16)

We demonstrate that α-aryl cyclic vinylo...

A Concise Total Synthesis of (-)-Mesembrine

Wang, Lu-Ning,Cui, Qi,Yu, Zhi-Xiang

, p. 10165 - 10171 (2016/11/17)

A concise total synthesis of mesembrine ...

Highly chemoselective aerobic oxidation of amino alcohols into amino carbonyl compounds

Sasano, Yusuke,Nagasawa, Shota,Yamazaki, Mai,Shibuya, Masatoshi,Park, Jaiwook,Iwabuchi, Yoshiharu

supporting information, p. 3236 - 3240 (2014/04/03)

The direct oxidation of unprotected amin...

Consecutive sigmatropic rearrangements in the enantioselective total synthesis of (-)-joubertinamine and (-)-mesembrine

Ilardi, Elizabeth A.,Isaacman, Michael J.,Qin, Ying-chuan,Shelly, Sommer A.,Zakarian, Armen

experimental part, p. 3261 - 3269 (2009/08/15)

Joubertinamine and mesembrine are two re...

24880-43-1 Process route

1-(3,4-dimethoxyphenyl)cyclopropanecarbaldehyde
20802-16-8

1-(3,4-dimethoxyphenyl)cyclopropanecarbaldehyde

methyl vinyl ketone
78-94-4,25038-87-3

methyl vinyl ketone

methylamine
74-89-5

methylamine

(-)-mesembrine
468-53-1,6023-73-0,21104-37-0,24880-43-1,28639-24-9,35056-46-3,35056-47-4

(-)-mesembrine

Conditions
Conditions Yield
1-(3,4-dimethoxyphenyl)cyclopropanecarbaldehyde; methylamine; With sodium sulfate; In 1,2-dichloro-ethane; at 20 ℃; for 0.166667h;
With chloro-trimethyl-silane; sodium iodide; In DMF (N,N-dimethyl-formamide); at 90 ℃; for 3h;
methyl vinyl ketone; With hydrogenchloride; more than 3 stages;
40%
1-(3,4-Dimethoxy-phenyl)-1-methyl-iminomethyl-cyclopropan
20802-17-9

1-(3,4-Dimethoxy-phenyl)-1-methyl-iminomethyl-cyclopropan

methyl vinyl ketone
78-94-4,25038-87-3

methyl vinyl ketone

(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
468-53-1

(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one

(-)-mesembrine
468-53-1,6023-73-0,21104-37-0,24880-43-1,28639-24-9,35056-46-3,35056-47-4

(-)-mesembrine

Conditions
Conditions Yield
1-(3,4-Dimethoxy-phenyl)-1-methyl-iminomethyl-cyclopropan; With chloro-trimethyl-silane; sodium iodide; In DMF (N,N-dimethyl-formamide); at 90 ℃; for 3h;
With hydrogenchloride; In diethyl ether; dichloromethane;
methyl vinyl ketone; With sodium hydroxide; more than 3 stages;

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