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Purity:99%
A series of 7-alkyl-3-benzylcoumarins wa...
2-methoxycinnamaldehyde
2-hydroxy-6-methoxy-4-pentylbenzaldehyde
PSB-SB-1202
| Conditions | Yield |
|---|---|
|
With
potassium carbonate; 1-methyl-3-methylimidazol-3-ium dimethyl phosphate;
In
toluene;
at 110 ℃;
for 0.833333h;
Inert atmosphere;
Microwave irradiation;
|
10% |
1,3-dimethoxy-5-pentylbenzene
PSB-SB-1202
| Conditions | Yield |
|---|---|
|
Multi-step reaction with 3 steps
1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / diethyl ether / 6 h / 0 - 20 °C
2: sodium iodide; aluminum (III) chloride / acetonitrile; dichloromethane / 1 h / 0 - 20 °C
3: potassium carbonate; 1-methyl-3-methylimidazol-3-ium dimethyl phosphate / toluene / 0.83 h / 110 °C / Inert atmosphere; Microwave irradiation
With
aluminum (III) chloride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; potassium carbonate; sodium iodide; 1-methyl-3-methylimidazol-3-ium dimethyl phosphate;
In
diethyl ether; dichloromethane; toluene; acetonitrile;
|
1,3-dimethoxy-5-pentylbenzene
2-methoxycinnamaldehyde
2-hydroxy-6-methoxy-4-pentylbenzaldehyde
2,6-dimethoxy-4-pentylbenzaldehyde
C21H22O4
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