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Purity:99%
A method for manufacturing a liquid crys...
PROBLEM TO BE SOLVED: To provide a metho...
4-(3-acryloyloxypropyloxy)benzoic acid
2-methylbenzene-1,4-diol
2-methylbenzene-1,4-diyl bis{4-[3-(acryloyloxy)propoxy]benzoate}
Conditions | Yield |
---|---|
4-(3-acryloyloxypropyloxy)benzoic acid;
With
methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; ethyl acetate;
for 1h;
Cooling with ice;
2-methylbenzene-1,4-diol;
With
1-methyl-1H-imidazole; triethylamine;
In
tetrahydrofuran; ethyl acetate;
at 20 ℃;
for 2h;
Cooling with ice;
|
2-methylbenzene-1,4-diol
C14H16O7S
2-methylbenzene-1,4-diyl bis{4-[3-(acryloyloxy)propoxy]benzoate}
Conditions | Yield |
---|---|
With
dmap; triethylamine;
In
tetrahydrofuran;
for 1h;
Cooling with ice;
|
12.3g |
4-(3-acryloyloxypropyloxy)benzoic acid
2-methylbenzene-1,4-diol
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