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pd_meltingpoint:232-234 °C(lit.)
Purity:99%
InChI:InChI=1/CH5N.ClH/c1-2;/h2H2,1H3;1H/i1D3;
Two perovskite-type compounds, (MA)2[B′C...
The present invention relates to a deute...
The invention discloses a method for pre...
The invention discloses a method for syn...
In recent years, several deuterated drug...
(N-(methyl-d3))-isoindole-1,3-dione instead of 2-(N-(methyl-d3))-isoindole-1,3-dione
methyl-d3-amine hydrochloride
Conditions | Yield |
---|---|
With
hydrogenchloride;
In
water;
at 105 ℃;
for 24h;
|
84.6% |
With
hydrogenchloride; water;
at 105 ℃;
|
80% |
With
hydrogenchloride;
In
water;
at 20 ℃;
Reflux;
|
80% |
With
hydrogenchloride;
In
water;
at 20 ℃;
Time;
Reflux;
|
80% |
With
hydrogenchloride;
In
water;
at 105 ℃;
|
80% |
With
hydrogenchloride;
In
water;
at 105 ℃;
for 24h;
|
56.9% |
With
hydrogenchloride;
In
water;
at 105 ℃;
for 48h;
|
51% |
With
hydrogenchloride;
In
water;
at 105 ℃;
for 48h;
|
51% |
With
hydrogenchloride;
In
water;
Reflux;
Sealed tube;
|
|
With
hydrogenchloride;
In
water;
Reflux;
Sealed tube;
|
C15H14(2)H3N
methyl-d3-amine hydrochloride
Conditions | Yield |
---|---|
With
hydrogenchloride; 10% palladium hydroxide on charcoal; palladium 10% on activated carbon; hydrogen;
In
methanol; water;
at 50 ℃;
for 24h;
under 760.051 Torr;
Reagent/catalyst;
|
93% |
N-Nitroso-N-methyl-d3-methoxymethylamine
(N-(methyl-d3))-isoindole-1,3-dione instead of 2-(N-(methyl-d3))-isoindole-1,3-dione
nitromethane-d3
methylamine hydrochloride
(1-benzyl-4-d3-methyl-piperidin-3-yl)-d3-methyl-amine
4-chloropyridinyl-2-(N-1',1',1'-trideuteromethylcarboxamide)
N-(4-chloro-3-(trifluoromethyl)phenyl)-N'-(4-(2-(N-(methyl-d3)aminoformyl)-4-pyridyloxy)phenyl)urea
2,4-dinitro-N-trideuteriomethyl-aniline
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