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Purity:99%
The racemic synthesis and subsequent res...
The present invention provides compounds...
The invention provides a synthesis metho...
Therapeutic compounds, and methods, comp...
5-methoxy-indan-1,2-dione 2-oxime
(±)-2-amino-5-methoxyindane
Conditions | Yield |
---|---|
5-methoxy-indan-1,2-dione 2-oxime;
With
sulfuric acid; hydrogen;
palladium 10% on activated carbon;
In
acetic acid;
for 18h;
under 3102.97 Torr;
With
sodium hydroxide;
In
water;
at 0 ℃;
pH=10;
|
37% |
5-methoxy-indan-1,2-dione 2-oxime;
With
sulfuric acid; hydrogen;
palladium 10% on activated carbon;
In
acetic acid;
for 18h;
under 3102.97 Torr;
With
sodium hydroxide;
In
water;
at 0 ℃;
pH=10;
|
37% |
With
sulfuric acid; hydrogen; acetic acid;
palladium on activated charcoal;
for 18h;
under 3102.97 Torr;
|
33% |
With
sulfuric acid; hydrogen;
palladium on activated charcoal;
In
acetic acid;
for 7h;
under 2585.74 Torr;
|
|
With
sulfuric acid; hydrogen;
10percent Pd/C;
In
acetic acid;
for 7h;
under 2585.81 Torr;
|
|
With
sulfuric acid;
palladium-carbon; palladium(II) chloride;
In
acetic acid;
|
|
With
sulfuric acid;
palladium-carbon; palladium(II) chloride;
In
acetic acid;
|
|
5-methoxy-indan-1,2-dione 2-oxime;
With
sulfuric acid; hydrogen; acetic acid;
palladium 10% on activated carbon;
under 2585.81 Torr;
With
sodium hydroxide;
|
5-(methyloxy)-2,3-dihydro-1H-inden-2-amine hydrochloride
(±)-2-amino-5-methoxyindane
Conditions | Yield |
---|---|
With
sodium hydroxide;
In
methanol; water;
at 0 - 25 ℃;
for 3h;
|
95% |
2-(hydroxyimino)-6-methoxy-2,3-dihydro-1H-inden-1-one
2-amino-6-methoxy-indan-1-ol; hydrochloride
5-methoxy-indan-1,2-dione 2-oxime
5-methoxy-1-indanone
5-(methyloxy)-2,3-dihydro-1H-inden-2-amine hydrochloride
2-(5-methoxyindane-2-yl)isoindole-1,3,dione
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