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Purity:99%
A convenient synthesis of drimenol by tr...
((1S,2R,4aS,8aS)-2-hydroxy-2,5,5,8a-tetramethyldecahydronaphthalen-1-yl)methyl acetate
albicanol
(-)-drimenol
![(+)-[(4aS,8aS)-2,5,5,8a-tetramethyl-3,4,4a,5,6,7,8,8a-octahydronaphthalen-1-yl]methanol](/upload/2025/4/0485d327-d87d-4096-bb1f-986dd49a217b.png)
(+)-[(4aS,8aS)-2,5,5,8a-tetramethyl-3,4,4a,5,6,7,8,8a-octahydronaphthalen-1-yl]methanol
| Conditions | Yield |
|---|---|
|
((1S,2R,4aS,8aS)-2-hydroxy-2,5,5,8a-tetramethyldecahydronaphthalen-1-yl)methyl acetate;
With
pyridine; trichlorophosphate;
at 20 ℃;
for 2h;
With
potassium hydroxide;
In
methanol;
at 20 ℃;
for 0.333333h;
Title compound not separated from byproducts;
|
4-methoxybenzene-1,3-diol
(+)-[(4aS,8aS)-2,5,5,8a-tetramethyl-3,4,4a,5,6,7,8,8a-octahydronaphthalen-1-yl]methanol
![4-methoxy-6-{[(4aS,8aS)-2,5,5,8a-tetramethyl-3,4,4a,5,6,7,8,8a-octahydronaphthalen-1-yl]methyl}benzene-1,3-diol](/upload/2025/4/6100841b-ed12-4478-a8e1-0729ccc3a0a6.png)
4-methoxy-6-{[(4aS,8aS)-2,5,5,8a-tetramethyl-3,4,4a,5,6,7,8,8a-octahydronaphthalen-1-yl]methyl}benzene-1,3-diol
| Conditions | Yield |
|---|---|
|
4-methoxybenzene-1,3-diol; (+)-[(4aS,8aS)-2,5,5,8a-tetramethyl-3,4,4a,5,6,7,8,8a-octahydronaphthalen-1-yl]methanol;
In
dichloromethane;
at 20 ℃;
for 0.0833333h;
Inert atmosphere;
With
boron trifluoride diethyl etherate;
In
dichloromethane;
at 20 ℃;
for 0.25h;
Inert atmosphere;
|
83% |
((1S,2R,4aS,8aS)-2-hydroxy-2,5,5,8a-tetramethyldecahydronaphthalen-1-yl)methyl acetate
2-Methyl-6-((4aR,4bS,8aS,10aR)-2,4b,8,8,10a-pentamethyl-3,4,4a,4b,5,6,7,8,8a,9,10,10a-dodecahydro-phenanthren-1-ylmethyl)-benzene-1,4-diol
(4aR*,4bS*,8aS*,10aR*)-1-<2,5-dihydroxy-3-methylbenzyl>-3,4,4a,4b,5,6,7,8,8a,9,10,10a-dodecahydro-2,4b,8,8,10a-pentamethylphenanthren-3-one
(4aR*,4bS*,8aS*,10aR*)-1-<2,5-bis(methoxymethoxy)-3-methylbenzyl>-3,4,4a,4b,5,6,7,8,8a,9,10,10a-dodecahydro-2,4b,8,8,10a-pentamethylphenanthrene
(4aR*.4bS*,8aS*,10aR*)-1-<2,5-bis(methoxymethoxy)-3-methylbenzyl>-3,4,4a,4b,5,6,7,8,8a,9,10,10a-dodecahydro-2,4b,8,8,10a-pentamethylphenanthrene-3-one
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