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Purity:99%
Synthesis Reference(s) |
Journal of the American Chemical Society, 69, p. 1911, 1947 DOI: 10.1021/ja01200a020Tetrahedron Letters, 16, p. 1731, 1975 |
InChI:InChI=1/C5H11NO2/c1-4(7)5(8)6(2)3/h4,7H,1-3H3
This disclosure relates to a method for ...
Provided are processes for making an ami...
Process for making an amide of a carboxy...
Novel ether-amide compounds are describe...
methyl lactate
dimethyl amine
2-hydroxy-N,N-dimethyl-propanamide
Conditions | Yield |
---|---|
With
methanol;
at 0 - 60 ℃;
for 20h;
Inert atmosphere;
|
60% |
at 70 ℃;
|
|
With
sulfuric acid;
at 20 - 30 ℃;
|
ethyl 2-hydroxypropionate
dimethyl amine
2-hydroxy-N,N-dimethyl-propanamide
Conditions | Yield |
---|---|
at 25 - 160 ℃;
for 16h;
Autoclave;
|
70% |
at 80 ℃;
for 20h;
Inert atmosphere;
|
52% |
With
methanol;
|
|
at 80 ℃;
|
ethyl 2-hydroxypropionate
dimethyl amine
methyl lactate
N,N-dimethyl-propanamide
DL-2-acetoxy-propionic acid dimethylamide
(R)-2-hydroxy-N,N-dimethylpropanamide
(S)-N,N-dimethyl lactamide
C11H21NO2
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