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pd_meltingpoint:159-160 °C(lit.)
Appearance:Off-white powder
Purity:99%
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Safety Profile |
Poison by subcutaneous route.Moderately toxic by ingestion and intraperitoneal routes.An experimental teratogen. Other experimentalreproductive effects. When heated to decomposition itemits acrid smoke and fumes. |
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Brand name |
Dolinac (Wyeth-Ayerst); Flexfree(Wyeth-Ayerst); Napageln (Wyeth-Ayerst); Target (Wyeth-Ayerst); Traxam (Wyeth-Ayerst). |
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General Description |
4-Biphenylacetic acid is a potential non-steroidal antiinflammatory agent and forms solid inclusion complex with β-cyclodextrin. 4-Biphenylacetic acid on interaction with quinolone antibacterial agents induces functional blockade of the γ-aminobutyric acid receptors. |
InChI:InChI=1/C14H12O2/c15-14(16)10-11-6-8-13(9-7-11)12-4-2-1-3-5-12/h1-9H,10H2,(H,15,16)/p-1
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4-biphenylacetonitrile
(4-biphenylyl)acetic acid
| Conditions | Yield |
|---|---|
|
With
water; potassium hydroxide;
In
ethylene glycol;
at 120 ℃;
for 16h;
|
97.6% |
|
With
hydrogenchloride;
|
|
|
With
water; sodium hydroxide;
for 4h;
Time;
Reflux;
|
|
|
With
sodium hydroxide;
In
water; butan-1-ol;
at 100 ℃;
for 8h;
Temperature;
|
biphenyl-4-methylchloride
carbon monoxide
(4-biphenylyl)acetic acid
| Conditions | Yield |
|---|---|
|
carbon monoxide;
With
C28H22CoN4O6;
In
butan-1-ol;
at 60 ℃;
for 2h;
under 760.051 Torr;
Glovebox;
High pressure;
Green chemistry;
biphenyl-4-methylchloride;
With
tetra-(n-butyl)ammonium iodide; sodium hydroxide;
In
butan-1-ol;
at 60 ℃;
for 22h;
under 760.051 Torr;
regioselective reaction;
Glovebox;
High pressure;
Green chemistry;
|
80% |
4-phenylmandelic acid
1,1-biphenyl-4-ylacetamide
acetoxy-biphenyl-4-yl-acetic acid ethyl ester
biphenyl
2-biphenyl-4-yl-5-phenyl-pent-2-en-4-ynoic acid
biphenyl-4-yl-acetyl chloride
cis-1-
cis-1-
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