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pd_meltingpoint:127-131 ºC
Appearance:COA
Purity:99%
|
Synthesis Reference(s) |
Tetrahedron, 48, p. 4301, 1992 DOI: 10.1016/S0040-4020(01)80441-5 |
InChI:InChI=1/C7H9NO/c8-5-6-3-1-2-4-7(6)9/h1-4,9H,5,8H2/p+1
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In this study, ten ω-transaminases (ω-TA...
This work includes an effective comparis...
Most current processes for the general s...
The invention discloses a method for syn...
2-[(6-chloro-pyridin-2-yl)-hydrazonomethyl]-phenol
6-chloropyridin-2-amine
2-Hydroxybenzylamine
| Conditions | Yield |
|---|---|
|
In
ethanol; water;
pH=2.3;
Further Variations:;
pH-values;
Kinetics;
Electrolysis;
|
salicylaldehyde-oxime
2-Hydroxybenzylamine
| Conditions | Yield |
|---|---|
|
With
(pyridine)(tetrahydroborato)zinc;
In
tetrahydrofuran;
for 0.5h;
Heating;
|
96% |
|
With
sodium tetrahydroborate;
at 20 ℃;
for 0.0333333h;
neat (no solvent, solid phase);
|
93% |
|
With
hydrogenchloride; hydrogen;
palladium on activated charcoal;
In
ethanol;
for 2h;
under 2844.3 Torr;
|
85% |
|
With
hydrogen;
palladium on activated charcoal;
In
methanol;
at 20 ℃;
for 4h;
under 672.292 Torr;
|
35% |
|
With
ammonia; sodium;
In
methanol;
|
|
|
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
for 2h;
|
|
|
Multi-step reaction with 2 steps
1: H2 / Raney-Ni
2: aq. HCl
With
hydrogenchloride; hydrogen;
nickel;
|
salicylonitrile
3,4-dihydro-2H-benzo[e][1,3]oxazin-2-one
salicylaldazine
(E)-2-hydroxylbenzaldehyde oxime
salicyl-urea
N-(2-hydroxybenzyl)salicylaldimine
2-aminomethyl-4,6-dibromo-phenol
salicylaldehyde
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