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pd_meltingpoint:56-57 °C
Purity:99%
InChI:InChI=1/C13H12O3/c1-10-13(12(14)7-8-15-10)16-9-11-5-3-2-4-6-11/h2-8H,9H2,1H3
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Maltol
benzyl chloride
3-O-benzylmaltol
| Conditions | Yield |
|---|---|
|
With
potassium carbonate;
In
acetonitrile;
for 5h;
Reflux;
|
99.4% |
|
With
potassium carbonate;
In
methanol;
for 1h;
Reflux;
|
98% |
|
With
triethylamine;
In
ethyl acetate;
Reflux;
|
98.2% |
|
With
sodium hydroxide;
In
methanol;
Heating / reflux;
|
95% |
|
With
sodium hydroxide;
In
methanol; water;
at 74.84 ℃;
|
95% |
|
|
94% |
|
With
sodium hydroxide;
In
methanol; dichloromethane; water;
|
94% |
|
With
sodium hydroxide;
In
methanol; water;
for 6h;
Product distribution / selectivity;
Heating / reflux;
|
94% |
|
With
sodium hydroxide;
In
methanol; water;
for 6h;
Heating;
|
92% |
|
With
sodium hydroxide;
In
methanol; water;
|
92% |
|
With
sodium hydroxide;
In
methanol;
for 8h;
Heating;
|
91% |
|
With
sodium hydroxide;
In
methanol; water;
for 8h;
Heating;
|
91% |
|
With
sodium hydroxide;
In
methanol; water;
for 18h;
Reflux;
|
88% |
|
With
sodium hydroxide;
In
ethanol; water;
at 60 ℃;
for 6h;
|
88% |
|
With
sodium hydroxide;
In
methanol; water;
for 12h;
Reflux;
|
87% |
|
With
sodium hydroxide;
In
methanol; water;
at 85 ℃;
for 2h;
|
87% |
|
With
sodium hydroxide;
In
methanol;
Reflux;
|
87% |
|
With
sodium hydroxide;
In
methanol;
Reflux;
|
86% |
|
With
sodium hydroxide;
In
methanol; water;
for 6h;
Heating;
|
85.6% |
|
With
sodium hydroxide;
In
methanol; water;
for 6h;
Heating;
|
85.6% |
|
With
sodium hydroxide;
In
methanol;
for 8h;
Reflux;
|
85.8% |
|
With
sodium hydroxide;
In
ethanol;
at 60 ℃;
for 6h;
Reflux;
|
85% |
|
With
sodium hydroxide;
In
methanol;
|
84% |
|
With
sodium hydroxide;
In
ethanol; water;
at 60 ℃;
|
84% |
|
With
sodium hydroxide;
In
methanol; water;
for 6h;
Heating;
|
83% |
|
With
sodium hydroxide;
In
methanol;
for 12h;
Heating;
|
83% |
|
Maltol;
With
sodium hydroxide;
In
methanol; water;
Reflux;
benzyl chloride;
In
methanol; water;
for 18h;
Reflux;
|
82% |
|
With
sodium hydroxide;
In
methanol; water;
for 8.5h;
Reflux;
|
82% |
|
Maltol;
With
sodium hydroxide;
In
methanol; water;
benzyl chloride;
In
methanol; water;
for 12.5h;
Heating;
|
82% |
|
With
sodium hydroxide;
In
methanol;
Heating;
|
81% |
|
Maltol;
With
sodium hydroxide;
In
methanol;
Reflux;
benzyl chloride;
for 0.5h;
Reflux;
|
81% |
|
With
sodium hydroxide;
In
methanol; water;
Reflux;
|
81% |
|
With
sodium hydroxide;
In
methanol; water;
Heating;
|
79% |
|
With
sodium hydroxide;
In
water;
for 40h;
Reflux;
|
79% |
|
With
sodium hydroxide;
In
ethanol; water;
at 60 ℃;
for 3.5h;
|
78% |
|
With
sodium hydroxide;
In
methanol; water;
|
76.8% |
|
With
sodium hydroxide;
In
methanol;
at 92 ℃;
for 22h;
|
69% |
|
With
sodium hydroxide;
In
methanol; water;
|
|
|
In
ethanol; water;
|
|
|
With
sodium hydroxide;
In
methanol;
at 65 ℃;
for 16h;
|
|
|
With
potassium hydroxide;
|
|
|
With
sodium hydroxide;
In
methanol;
Reflux;
|
|
|
With
sodium hydroxide;
In
methanol; water;
for 6h;
Reflux;
|
|
|
In
methanol; water;
Reflux;
Alkaline conditions;
|
|
|
With
sodium hydroxide;
In
methanol; water;
for 20h;
Reflux;
|
Maltol
benzyl chloride
1-acetyl-3-hydroxy-2-methylpyrid-4-one 3-Benzyloxy-2-methyl-4-pyrone
3-O-benzylmaltol
| Conditions | Yield |
|---|---|
|
With
sodium hydroxide;
In
methanol; water;
|
92% |
Maltol
benzyl bromide
benzyl chloride
4-(((2-methyl-4-oxo-4H-pyran-3-yl)oxy)methyl)phenylboronic acid
3-Benzyloxy-2-methyl-1-(propyl)-pyridin-4(1H)-one
1,1'-(hexane-1,6-diyl)bis(3-(benzyloxy)-2-methylpyridin-4(1H)-one)
3-Benzyloxy-2-methyl-1-octyl-1H-pyridin-4-one
3-(benzyloxy)-1-hexyl-2-methylpyridin-4(1H)-one
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