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pd_meltingpoint:121-122 °C
Purity:99%
|
Synthesis Reference(s) |
Journal of the American Chemical Society, 105, p. 2382, 1983 DOI: 10.1021/ja00346a046Tetrahedron Letters, 27, p. 5019, 1986 DOI: 10.1016/S0040-4039(00)85122-9 |
InChI:InChI=1/C5H8N2/c1-4-5(2)7-3-6-4/h3H,1-2H3,(H,6,7)
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formaldehyd
dimethylglyoxal
4,5-dimethylimidazole
2,4,5-trimethyl-1H-imidazole
| Conditions | Yield |
|---|---|
|
With
ammonia; water;
|
formaldehyd
dimethylglyoxal
4,5-dimethylimidazole
| Conditions | Yield |
|---|---|
|
With
ammonium sulfate;
In
water;
for 1h;
Reagent/catalyst;
Reflux;
|
69% |
|
formaldehyd;
With
ammonium bisulphate;
In
water;
at 20 ℃;
for 0.0833333h;
dimethylglyoxal;
In
water;
for 1.66667h;
Reflux;
|
68% |
|
With
ammonia;
In
water;
at 20 ℃;
for 1h;
|
4,5-dimethylimidazole-2(3H)-thione
ethyl nitrite
4,5-dimethyl-oxazole
formamide
2-(p-bromophenylazo)-4,5-dimethylimidazole
1-benzoyl-4,5-dimethyl-1H-imidazole
2-methyl-3H-imidazole-4-carboxylic acid
2-chloro-5,6-dimethylpyrazine
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