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pd_meltingpoint:121-122 °C (decomp)
Purity:99%
|
Safety Profile |
Poison by ingestion andsubcutaneous routes. Questionable carcinogen withexperimental tumorigenic data. Mutation data reported.When heated to decomposition it emits toxic fumes ofNOx and F-. |
InChI:InChI=1/C6H5N2.BF4/c7-8-6-4-2-1-3-5-6;2-1(3,4)5/h1-5H;/q+1;-1
Five organic redox systems were examined...
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Given their ubiquity in natural products...
tetrafluoroboric acid
aniline
benzenediazonium tetrafluoroborate
| Conditions | Yield |
|---|---|
|
With
sodium nitrite;
In
water;
at 0 ℃;
for 3h;
|
99.5% |
|
tetrafluoroboric acid; aniline;
In
ethanol; water;
at 20 ℃;
for 0.0333333h;
With
tert.-butylnitrite;
In
ethanol; water;
at 0 - 20 ℃;
for 1.25h;
|
98% |
|
tetrafluoroboric acid; aniline;
In
ethanol; water;
for 0.25h;
With
sodium nitrite;
In
ethanol; water;
at 0 ℃;
for 1h;
|
98% |
|
With
sodium nitrite;
In
water;
at 0 ℃;
for 1h;
Inert atmosphere;
|
93% |
|
With
sodium nitrite;
In
water;
at -7 - 1 ℃;
for 2h;
|
87% |
|
With
sodium nitrite;
In
water;
at 0 - 5 ℃;
for 2h;
|
86.6% |
|
With
sodium nitrite;
In
water;
for 0.166667h;
|
86.7% |
|
aniline;
With
hydrogenchloride; sodium nitrite;
In
water;
at 0 ℃;
for 0.5h;
tetrafluoroboric acid;
In
water;
at 0 ℃;
Cooling with ice;
|
85% |
|
With
tert-butyl methyl ether; sodium nitrite;
In
water;
at 0 - 20 ℃;
for 0.833333h;
Inert atmosphere;
|
80% |
|
tetrafluoroboric acid; aniline;
In
water;
at 0 ℃;
for 1h;
With
sodium nitrite;
In
water;
for 1h;
|
76% |
|
With
sodium nitrite;
In
water;
at 0 ℃;
for 1h;
|
74% |
|
With
sodium nitrite;
In
water;
at 0 ℃;
for 0.5h;
|
70% |
|
tetrafluoroboric acid; aniline;
In
water;
at 0 ℃;
With
sodium nitrite;
In
water;
at 0 ℃;
for 0.5h;
|
60% |
|
With
sodium nitrite;
In
water;
at 0 ℃;
for 0.666667h;
|
49% |
|
With
sodium nitrite;
In
water;
at -5 - 0 ℃;
for 0.666667h;
|
|
|
With
sodium nitrite;
In
water;
for 0.5h;
Cooling with ice;
|
|
|
With
sodium nitrite;
In
water;
for 0.5h;
Cooling with ice;
|
|
|
With
sodium nitrite;
In
water;
at 0 ℃;
|
|
|
With
sodium nitrite;
In
water;
at 0 ℃;
for 3.33333h;
|
|
|
With
tert.-butylnitrite;
In
ethanol; water;
at 0 - 20 ℃;
for 1h;
|
|
|
With
sodium nitrite;
In
water;
at 0 ℃;
for 0.666667h;
Inert atmosphere;
Schlenk technique;
|
|
|
With
sodium nitrite;
In
water;
at 0 ℃;
for 0.666667h;
|
|
|
With
sodium nitrite;
In
water;
for 0.5h;
Cooling with ice;
|
|
|
With
tert.-butylnitrite;
In
ethanol; water;
at 0 - 20 ℃;
for 1h;
|
|
|
With
sodium nitrite;
In
water;
at 0 ℃;
for 1h;
|
|
|
tetrafluoroboric acid; aniline;
In
ethanol; water;
at 20 ℃;
for 0.0833333h;
With
tert.-butylnitrite;
In
ethanol; water;
at 0 ℃;
for 2h;
Inert atmosphere;
|
|
|
With
sodium nitrite;
In
water;
at 0 ℃;
for 0.5h;
|
boron trifluoride diethyl etherate
aniline
benzenediazonium tetrafluoroborate
| Conditions | Yield |
|---|---|
|
With
tert.-butylnitrite;
In
dichloromethane;
at 0 - 20 ℃;
for 1h;
Inert atmosphere;
|
95% |
|
With
tert.-butylnitrite;
In
dichloromethane;
at 0 - 20 ℃;
for 2h;
|
|
|
With
tert.-butylnitrite;
In
methanol;
at -20 - 20 ℃;
Inert atmosphere;
|
phenylhydrazine hydrochloride
aniline
phenylhydrazine
N-trimethylsilylaniline
benzene
2-methyl-N-phenylbenzamide
fluorobenzene
phenyl radical
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